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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 29, Number 3
JKCSEZ 29(3)
June 20, 1985 

 
Title
Synthesis of 1-[3-(Propylthio)butyryl]-2,6,6-trimethylcyclohexene

1-[3-(프로필티오) 부티릴]-2,6,6-트리메틸시클로헥센의 합성
Author
Jong Hoon Oh, Kyongtae Kim, Yong Tae Kim

오종훈, 김경태, 김용태
Keywords
Abstract
2,6,6-trimethylcyclohex-l-en-1-yllithium (9)과 3-propylthiobutyraldehyde (16)의 반응으로 부터 1-[3-(Propylthio)butyryl]-2,6,6-trimethylcyclohexene (18)을 합성하였다. 이 방법을 이용하여 강력한 향료로 알려진 1-[3-(methylthio)butyryl]-2,6,6-trimethylcyclohexene (1)을 합성할 것이다.

1-[3-(Propylthio)butyryl]-2,6,6-trimethylcyclohexene (18) was synthesized from the reaction of 2,6,6-trimethylcyclohex-l-en-1-yllithium (9) with 3-propylthiobutyraldehyde (16). This method will be employed to prepare 1-[3-(methylthio)butyryl]-2,6,6-trimethylcyclohexene (1) which is known as one of the powerful flavors and fragrances.

Page
311 - 318
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