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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 19, Number 6
JKCSEZ 19(6)
December 20, 1975 
 
Title
 A Study on the Tungsten (Ⅵ) Complexes with the Organic Acid Anhydrides

유기산 무수물을 리간드로한 텅스텐 (Ⅵ) 착물에 관한 연구
Author
 Sang-Oh Oh, Chan-Ho Kim

오상오, 김찬호
Keywords
Abstract
 Oxygen doner인 무수유기산을 가진 dichloro-dioxo tungsen(VI) 착물의 합성방법을 연구하였다. RCOCl과 NaWO4를 반응시켜서 일반식 WO2Cl2(RCO)2O로 표시할 수 있는 황색분말인 단핵착물을 합성하고 그 성질을 고찰하였다. 이 새로운 착물의 구조를 스펙트럼과 화학적인 방법에 의하여 측정하였다.

Dichloro-dioxo-tungsten(Ⅵ) complexes containing oxygen donor in anhydrous organic acid have been synthesized. Sodium tungstate reacts with acetylchlorides to produce the mononuclear complexes, yellow powder having WO2Cl2(RCO)2O as general formula. Their chemical properties and the possible structure are proposed by the results of spectral data and chemical observation.
Page
 408 - 413
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