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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 11, Number 1
BKCSDE 11(1)
January 20, 1990 
 
Title
 Crystal Structure of Bithionol, C12H6Cl4O2S
Author
 Hyun Song, Euisung Kim, Hyun-So Shin*
Keywords
Abstract
 The crystal structure of Bithionol, C12H6Cl4O2S, has been determined from X-ray intensity data measured by Enraf-Nonius CAD-4 diffractometer using graphite-monochromatized Mo-Kα radiation. The crystal data as follows; triclinic space group P1, a = 8.879(2), b = 10.782(1), c = 8.511(1)Å, α = 115.43(1), β = 115.22(1), γ = 74.44°(1). μ = 9.51 cm-1, F(000) = 356, Z = 2. Final R value is 0.036 for independent 2669 observed reflections. Each six-membered benzene rings are coplanar within experimesntal errors and the dihedral angle between these planes is 81.28 ° (1). The S-(1) and S-C(7) distances are 1.787(2) and 1.791(3)Å, respectively.
Page
 19 - 21
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