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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 6, Number 3
BKCSDE 6(3)
March 20, 1985 

 
Title
Synthesis and 1H-nmr of N-Arylated Nitrogen-Containing Aromatic Heterocycles
Author
Kwanghee Koh Park, Jaebong Lee, Duhee Han
Keywords
Abstract
N-Arylation reaction of nitrogen-containing heterocycles such as pyridine, nicotinamide and 4,4'-bipyridine was studied. We prepared N-2,4-dinitrophenyl derivatives initially by reacting the above heterocycles with 2,4-dinitrochlorobenzene in ethanol, and then treated the N-2,4-dinitrophenylated heterocycles with various aniline derivatives, XC6H4NH2(X = -H, p-CH3, p-C2H5, p-Cl, p-CN, p-OH, p-OCH3, o-Cl, m-CH3) to yield the corresponding N-arylated compounds in fairly good yields. H1-nmr patterns and peak assignments of the N-arylated products were described.
Page
141 - 144
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