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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 14, Number 1
JKCSEZ 14(1)
February 20, 1970 

Studies on the Crystal Structure of Benzidine Perchlorate by X-ray Diffraction method (Ⅱ) Crystal Structure Analysis

X-선 회절법을 이용한 벤지딘과염소산염의 결정구조에 관한 연구 (Ⅱ) 결정구조의 해석
Chung Hoe Koo, Hyun So Shin, Man Hyong Kang

구정회, 신현소, 강만형
The approximate crystal structure of benzidine monoperchlorate has been determined by single crystal X-Ray diffraction technique and patterson method. As the molecule has a center of symmetry in it and location of perchlorate ion is symmetrically on the mirror plane in the unit cell, perchlorate ion is forming hydrogen bond with two -NH2 groups in the different molecule. Thus, one molecule of benzidine and perchloric acid combines 1:1 by mole ratio.
123 - 126
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