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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 61, Number 4
JKCSEZ 61(4)
August 20, 2017 

 
Title
One Pot Four-Component Synthesis of Novel Substituted 2-Phenyl-4(3H) Quinazolinones Using Recyclable Nanocrystalline CuMnO3 Catalyst
Author
A V Borhade*, D R Tope, G D Gare, G B Dabhade
Keywords
Green synthesis, Mixed metal oxide, Multicomponent reaction, 2-Phenyl-4(3H) quinazolinone, Recyclable catalyst
Abstract
In the present study, nanocrystalline mixed metal oxide, CuMnO3 catalyst have been synthesized by mechanochemical method with green chemistry approach. The synthesized catalyst was characterized by analytical techniques including FTIR, XRD, SEM, TEM and BET surface area. The synthesized catalyst shows high surface area is 121.06 m2/g with particle size 18 nm. The one pot four component synthesis of substituted 2-phenyl-4(3H) quinazolinone from the reaction of anthranilic acid, benzoyl chloride, hydrazine hydrate and substituted benzaldehyde in presence of CuMnO3 nanocatalyst has been carried out. It affords the corresponding products with high yield (76-95%) in very short reaction time. All the obtained products were characterized with 1HNMR, 13CNMR, FTIR and EIMS.
Page
157 - 162
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