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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 57, Number 5
JKCSEZ 57(5)
October 20, 2013 

 
Title
Fabrication and Characterization Nano Porous Anodic ZrO2 Membranes by Two-Step Anodizing

2 단계 양극 산화를 이용한 ZrO2 나노 다공성 산화막의 제조와 특성에 관한 연구
Author
Eui Young Seo, Se Kyeong Choi, Ik Soo Shin*, Wee Kyung Kang*

서의영, 최세경, 신익수*, 강위경*
Keywords
Electrochemistry, Nano-porous oxide film, Anodizing, ZrO2
Abstract
Zirconium oxide (ZrO2) nano porous membranes were fabricated by electrochemical two-step anodization with an electropolished zirconium substrate in inorganic water-based and organic electrolyte systems containing small amounts of fluoride. Using two-step anodization and organic electrolytes, highly regular and ordered nanotubular ZrO2 oxide layers can be compared with aqueous electrolytes. The morphology and size of the nano porous layers were characterized by FE-SEM (field emission scanning electron microscopy), XRD (X-ray diffraction), and EDS (energy dispersive spectroscopy). Luminescence properties were investigated by photoluminescence measurements.
Page
547 - 553
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