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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 52, Number 5
JKCSEZ 52(5)
October 20, 2008 

A Simple and Efficient Grindstone Chemistry Solid-state Reaction Procedure for the Synthesis of Heterocyclic Oximes in Dry Media

무수조건하에서 헤테로 옥심의 합성을 위한 간단하고 효율적인 맷돌화학 고체상태의 반응과정
M. Gopalakrishnan*, J. Thanusu, V. Kanagarajan

M. Gopalakrishnan*, J. Thanusu, V. Kanagarajan
Oximation, 활성화된 비산회, 맷돌 화학, 녹색 화학 , Oximation, Activated Fly Ash, Grindstone Chemistry, Green Chemistry
무수조건하에서 막자와 막자사발을 이용하여 활성화된 비산회 촉매로 3-alkyl-2,6-diarylpiperidins, tetrahydrothiopyrans 과 tetrahydropyran-4-ones의 다양한 다른 헤테로 옥심을 합성하였고, 녹는점, 원소 분석, MS, FT-IR 그리고 1H NMR 데이터로 구조 분석하였다.

Various diverse heterocyclic oximes of 3-alkyl-2,6-diarylpiperidins, tetrahydrothiopyrans, and tetrahydropyran-4-ones are synthesized using a mortar and pestle in dry media catalyzed by activated fly ash in excellent yields and are characterized by melting point, elemental analysis, MS, FT-IR, and 1H NMR spectroscopic data.

523 - 529
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