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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 51, Number 4
JKCSEZ 51(4)
August 20, 2007 

 
Title
One-pot Synthesis of 5,7-Diaryl-3,4,6-trihydronaphthalen-2-ones

5,7-Diaryl-3,4,6-trihydronaphthalen-2-ones의 One-pot 합성
Author
M. Gopalakrishnan*, H. Manikandan, P. Sureshkumar, J. Thanusu, V. Kanagarajan

M. Gopalakrishnan*, H. Manikandan, P. Sureshkumar, J. Thanusu, V. Kanagarajan
Keywords
3,5-Diarylcyclohex-2-en-1-ones, Methyl vinyl ketone, Sodium ethoxide, One-pot, 5,7-Diaryl-3,4,6-trihydronaphthalen-2-ones. , 3,5-Diarylcyclohex-2-en-1-ones, Methyl Vinyl Ketone, Sodium Ethoxide, One-pot, 5,7-Diaryl-3,4,6-trihydronaphthalen-2-ones
Abstract
sodium ethoxide의 존재하에서 3,5-diaryl-cyclohex-2-en-1-one와 methyl vinyl ketone로부터 5,7-Diaryl- 3,4,6-trihydronaphthalen-2-ones가 합성되었다. 이 생성물은 IR, UV-Visible, 1H-NMR, 13C-NMR 그리고 mass spectral techniques로 구조를 규명하였다. 1H과 13C signals의 피크들은 HSQC spectrum을 찍어 정확히 규명하였다.

5,7-Diaryl-3,4,6-trihydronaphthalen-2-ones have been synthesized from 3,5-diaryl-cyclohex-2-en-1- ones and methyl vinyl ketone in the presence of sodium ethoxide. The products were characterized by IR, UV-Visible, 1H-NMR, 13C-NMR and mass spectral techniques. To confirm 1H and 13C signals, HSQC spectrum was recorded and analyzed.

Page
356 - 360
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