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Journal of the Korean Chemical Society (JKCS)

ISSN 1017-2548(Print)
ISSN 2234-8530(Online)
Volume 51, Number 2
JKCSEZ 51(2)
April 20, 2007 

 
Title
Synthesis of Aminofuroxan Derivatives for the Alkyne Formation on Solid Surface and e-Beam Mediated Fragmentation in Gas Phase

고체상 표면에서 알카인 생성을 위한 아미노퓨록산 유도체의 합성과 전자빔에 의한 기체상 분해반응
Author
Jeong-Mu Heo, Gi Young Kim, Kwang-Jin Hwang*

허정무, 김기영, 황광진*
Keywords
알카인, 퓨록산, 전자빔, 분해반응 , Alkyne, Furoxan, e-beam, Fragmentation
Abstract
고체상 표면에서 퓨록산 화합물의 박막생성을 위하여 클로로퓨록산 2와 butyl 및 benzyl amine과 반응시킨 아미노퓨록산 3,4를 합성하고 이들 아미노퓨록산 화합물을 질량분석기에서 전자빔에 의한 분해반응을 분석하여 알카인의 생성에 대한 효율성을 살펴보았다.

Aminofuroxan derivatives 3 and 4 were prepared by the reaction of chlorofuroxan 2 with butyl and benzyl amines, respectively. E-beam mediated fragmentation of aminofuroxans 3, 4 in mass spectrometer was analyzed in a view of the corresponding alkyne formation.

Page
160 - 164
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