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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 19, Number 7
BKCSDE 19(7)
July 20, 1998 

The Priparation of Alkenyl Fluorides from Organometallic Reagents
Seung-Han Lee, Martin Riediker, Jeffrey Schwartz
Fluorination of alkenyllithium reagents can be accomplished in acceptable yield under conditions which give rise to low competitive alkene formation. These reactions are abetted by the use of the low temperature soluble, mild fluorinating agent N-fluoro-N-tert-butylbenzenesulfonamide; "simpler" fluorinating reagents such as F2, XeF2 or FClO3 failed to give acceptable amounts of the fluoroolefin with these alkenyllithiums.
760 - 766
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