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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 16, Number 11
BKCSDE 16(11)
November 20, 1995 

 
Title
Syntheses and Characterizations of Lactam Cyclophanes. Attempted Synthesis of a Lactam Catenane Using Hydrogen Bonds
Author
Kyungmi Joo, Hyejae Ihm, Kyungsoo Paek*
Keywords
Abstract
New cyclophanes having multilactam linkages were synthesized and characterized. One-pot coupling reaction of 2,6-pyridinedicarbonyl dichloride and a diamine gave a tetralactam, a hexalactam, and a octalactam in good yields. The TLC behaviour, the molecular symmetry shown by 1H NMR spectrum, and the fragmentation patterns shown by FAB mass spectrum of the octalactam support its monocyclic structure.
Page
1079 - 1084
Full Text
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