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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 13, Number 5
BKCSDE 13(5)
May 20, 1992

Title	Synthesis of Tetradecker Sandwich Complex with 1,4-Dialkyl-1,4-dibora-2,5-cyclohexadiene
Author	Jae-Kook Uhm*, Walter Siebert
Keywords
Abstract	A tetradecker sandwich compiex (7a) was synthesized in low yield by the reaction of a tripledecker, bis(η5-cyclopentadienyl)-μ-(η 6-1,2,3,4-tetramethyl 1,4-dibora-2,5-cyclohexadiene) dinickel (5a) with potassium and FeCl2·2THF. The reaction of another tripledecker, bis(η5-cyclopentadienyl)-μ-(η 6-2,3-diethyl-1,4-dimethyl-1,4-dibora-2,5-cyclohex adiene) dicobalt (4a) with potassium and FeCl2· 2THF at room temperature produced a doubledecker complex (2b) via the decomposition of the dark green crystal.
Page	528 - 530
Full Text	PDF

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