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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 13, Number 4
BKCSDE 13(4)
April 20, 1992 

Preparation and Structure of CH2CH2OOCCHCH2SnCl3
Ok-Sang Jung, Young-A Lee, Jong Hwa Jeong, Youn Soo Sohn*
A new estertin, CH2CH2OOCCHCH2SnCl3, was prepared and its structure was determined by X-ray crystallography (P212121; a = 9.439(l), b = 9.601(l), c = 10.779(l) Å, Z = 4) and refined to R = 0.0356. The coordination geometry around the tin atom approximates to a trigonal bipyramid with the intramolecularly coordinated oxygen O(1), (Sn-O(1), 2.482(6)Å) and Cl(2) occupying mutually trans positions (O(1)-Sn-Cl((2), 176.4(2)°).
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