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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 6, Number 6
BKCSDE 6(6)
June 20, 1985 

 
Title
Reactions of Thianthrene Catio Radical Perchlorate with Azo-bis-2-phenoxy-2-propane and Azo-bis-2-(p-nitrophenoxy)-2-propane
Author
Jae Moon Lee, Kyongtae Kim, Jung Hyu Shin
Keywords
Abstract
Thianthrene cation radical perchlorate (1) reacted with azo-bis-2-phenoxy-2-propane (6) to give thianthrene (2), cis-thianthrene-5,10-dioxide, 5-(p-hydroxyphenyl) thianthrenium perchlorate (10), acetone, phenol, and 5-(2-propenyl) thianthrenium perchlorate (11) when the mole ratio of 1 to 6 was 1:1. Among the products, 11 was a new compound. However, when the corresponding mole ratio was 5:1, 11 was not formed. Similar result was obtained for azo-bis-2-(p-nitrophenoxy)-2-propane.
Page
358 - 361
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