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Bulletin of the Korean Chemical Society (BKCS)

ISSN 0253-2964(Print)
ISSN 1229-5949(Online)
Volume 5, Number 1
BKCSDE 5(1)
January 20, 1984 

 
Title
Synthesis of Nucleophilic Adducts of Thiols (Ⅴ). Addition of Thioglycolic Acid to ω, ω-Diacetylstyrene Derivatives
Author
Tae-Sung Huh, Hae-Sook Han, In-Sup Han, Tae-Rin Kim
Keywords
Abstract
The addition reactions of thioglycolic acid to ω, ω-diacetylstyrene derivatives were investigated. ω, ω-Diacetylstyrene derivatives easily undergo addition reactions with thioglycolic acid to form s-(2, 2-diacetyl-1-phenylethyl)-thiogycolic acid, s-[2,2-diacetyl-1-(methyl) phenylethyl]-thioglycolic acid, s-[2,2-diacetyl-1-(p-methoxy) phenylethyl]-thioglycolic acid and s-[2,2-diacetyl-1-(p-chloro) phenylethyl]-thioglycolic acid, respectively. The structures of these compounds were identified by neutralization equivalent, UV, IR, and NMR spectral data.
Page
21 - 23
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